Procedure – Powder/Chip Samples

Prepare the instrument as outlined in the operator's instruction manual.

Login a minimum of three Blank reps.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

氧氮?dú)浞治鰞x的原理：分析樣品在惰性氣流存在下于石墨坩堝中加熱熔融，其中脈沖爐溫度可自由設(shè)定，并通過(guò)一個(gè)非接觸式的光學(xué)溫度傳感器進(jìn)行實(shí)時(shí)監(jiān)控，用于實(shí)現(xiàn)樣品的完全分解，反應(yīng)所生成的CO H2和N2被帶入到具有高穩(wěn)定性和靈敏度的檢測(cè)系統(tǒng)進(jìn)行檢測(cè)。對(duì)于CO的檢測(cè)采用的是非色散性紅外檢測(cè)器，對(duì)于N2和H2的檢測(cè)則采用熱導(dǎo)檢測(cè)器。

氧氮?dú)浞治鰞x的特點(diǎn)：快速準(zhǔn)確分析，自動(dòng)化操作；精密氣體校準(zhǔn)；CO紅外檢測(cè)器，高分辨率和重現(xiàn)性的N、H熱導(dǎo)池檢測(cè)器；同一臺(tái)儀器實(shí)現(xiàn)熔融提取和熱提取；熱提取分析時(shí)間可調(diào)；可自由選擇溫度*高達(dá)2500 °C；光學(xué)溫度計(jì)溫度測(cè)定和控制；所有檢測(cè)器自動(dòng)調(diào)零/自動(dòng)水平控制（ALC）；數(shù)據(jù)評(píng)估的自動(dòng)優(yōu)化選擇范圍；爐自動(dòng)清潔和坩堝自動(dòng)進(jìn)樣（可選）；外設(shè)電腦進(jìn)行操作和控制；樣品信息保存； 所有樣品數(shù)據(jù)可追蹤查詢；通過(guò)FTP或本地局域網(wǎng)進(jìn)行數(shù)據(jù)傳輸； ON，H分析輕松切換。

山西氧氮?dú)浞治鰞x優(yōu)惠價(jià)格通用下電極坩堝支座，容納各種坩堝使用。

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Add approximately 0.05 g of *** Graphite Powder to a***Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen,the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 3b through 3i a minimum of three times for each calibration/drift standard used.

Summary

The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high

mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power

electrode furnace to quickly and efficiently release the target gases from within the sample, which allows

for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

Cornerstone氧氮?dú)浞治鲕浖瑫r(shí)支持***的數(shù)據(jù)文檔格式和可變的報(bào)告格式。

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

Oxygen and nitrogen are alloying elements in titanium, and are also classified as alpha stabilizing elements as they promote alpha phase alloys. Interstitial oxygen and nitrogen levels can be used to regulate the tensile strength of the material, but due to its high solubility can cause unwanted surface embrittlement. This phenomenon can be leveraged,however, under controlled processing to create surface films that increase surface hardness and wear properties.

***觸摸屏技術(shù)，用戶友好界面軟件進(jìn)行校正、分析、診斷等。山西氧氮?dú)浞治鰞x優(yōu)惠價(jià)格

Procedure - Solid Samples

Instrument calibration/drift correction.

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.

Calibrate/drift following the procedure outlined in the operator's instruction manual.